Advances In Chemical Propulsion, Science To Technology by Roy,G D Ed

By Roy,G D Ed

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The reactive intermediate(s) generated were trapped in situ by cyclohexene. Careful integration of the gated-decoupled 13 C NMR spectrum of 13 — 13 C obtained indicated that no scrambling of the 13 C label had occurred in the product. This result contradicts the incursion of 12b as an intermediate in this reaction [18].

1-Azidonorborniane was synthesized according to a modified literature procedure shown in Fig. 11. 4 SYNTHESIS OF QUADRICYCLANES Quadricyclane is a strained molecule which is relatively easy to synthesize. The strain energies of related structures are presented in Fig. 12. The aim of this part of the study was to incorporate the azido group into the strained quadricyclane structure. The pathways shown in Fig. 13 were pursued. Reaction 7 −→ 9 is general for synthesis of bridgehead azides of bridged polycyclic hydrocarbons.

It has been shown that the blow-off limit of premixed jet flame can be extended by an order of magnitude by the technique, thus providing a practical means for increasing the range of operation of propulsion devices. Several techniques have been investigated, with and without swirl, to control the pressure oscillations in combustion that are detrimental to performance, and may even cause failure and breakdown. James Whitelaw and his group at Imperial College of Science, Technology and Medicine, London, actively controlled the pressure oscillations in two models of lean-burn gas turbine combustors through oscillations in the fuel flow (Chapter 19).

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